In 1969 this laboratory had prepared 131 mc. of radiopharmaceuticals in total (Hippuran and other four kinds) and distributed to the major medical establishment. The quality and stability of these products were reviewed by means of radio paper partition chromatography and thin layer chromatography and results were compared to those of foreign products. Generally, the quality and stability of the product of this laboratory were better than those of the foreign product, even though the properties of the radiopharmaceutical were varied by the procedure of the preparation adopted. Various precautions for handling radiopharmaceuticals for clinical use were also described with a view of quality control and stability test there of.