The iodine containing radiopharmaceuticals, Hippuran, L- Thyroxine, Triiodothyronine, Rose Bengal, RISA, MAA, Triolein, Oleic acid and sterilized iodide solution were prepared. The labelling yield was av. 100-70%. The exchange method, iodination method, and chloramine-T procedure for a low temperature iodination were adopted as the preparative procedures. The preparative procedures and pyrogen free test of products were described and the distribution activity of the products in this institute was reported.